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raman:start [2011/05/06 16:41] – janet | raman:start [2020/09/25 11:13] (current) – janet | ||
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====== Raman Spectroscopy ====== | ====== Raman Spectroscopy ====== | ||
- | Raman spectrometer: | + | Raman spectrometer: |
- | Point person: Jason Francis (PH), Debra Gale (Rorrer group), Tristan deBorde (Minot group). | + | |
- | Scheduling: | + | |
- | Manuals: | + | |
- | ===== Scheduling ===== | + | |
- | [[< | + | |
- | <iframe src=" | + | Point person: Okan Agirseven < |
- | https://www.google.com/calendar/embed?src=vnulafmhvq4jegpmh76cp1nbt0%40group.calendar.google.com& | + | ==Manuals: |
+ | Horiba THMS600 heating stage manual {{: | ||
+ | |||
+ | ==Helpful resources== | ||
+ | * [[http://www.horiba.com/us/en/ | ||
+ | |||
+ | ===== Scheduling ===== | ||
+ | Please schedule your Raman usage. This allows you to reserve a spot, and also allows us to track the usage. | ||
[[https:// | [[https:// | ||
+ | |||
+ | ===== Pointers (8/2014) ===== | ||
+ | 1) Please be gentle with the switch to change between the 532 and 785 lasers, moving it carefully and slowly.Carelessly throwing the switch back and forth causes the mirrors to become misaligned and lower the quality of your data. | ||
+ | |||
+ | 2) Don't mess with the AC. Thermal expansion can also be a cause for alignment issues(again, | ||
+ | |||
+ | 3) Please note changes in the laser power if you use the fine tune knob on the 532nm laser. | ||
+ | |||
+ | 4) Please save all data in your folder and not just on the desktop. All files on the desktop will periodically be placed in a " | ||
+ | |||
+ | 5) If the Raman camera does not work, then try restarting the computer - it could be a software issue. | ||
+ | |||
+ | 6) Make sure to record the position and intensity (# counts) of the reference Si calibration peak every time calibration file on the Raman computer desktop. Also your name and the date. This helps to track the system folder. 65,000 to 70,000 counts is high; more usually 45,000. Should be at 520 cm^-1, can vary to 518-523 cm^-1 (temperature? | ||
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+ | 7) Usual Raman mode is 3s accumulation and 3 times at each energy. Can increase time and frequency. | ||
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