Using Icon-NMR software to automate 1H NMR experiment on the Bruker 400 MHz instrument.  Experimental Chemistry II, CH 463/H
Weigh or dispense about 10 - 20 mg of sample into a 4/5 dram vial.
	Measure about 3/4 mL of solvent using a disposable pipet.  It should look like about this much.
Pipette solvent into vial and draw mixture back and forth until a solution is made.
	Dispense solution using pipette into the NMR tube.  The depth of solution should be about 3 cm.
The tube is then fitted with the spinner, and tube and spinner are placed into the depth gauge.  This puts the spinner at the correct height.	Spinner (left) and depth gauge (right)
After depth gauging it, the tube should look like this fitted with the spinner
Carefully put the sample tube in the probe chamber on top of the magnetic
	The sample should look like this in the chamber.
Load ICON-NMR on the computer console for the Bruker 400 FTNMR system in Gilbert 228.  Consult the directions for using ICON-NMR (separate handout.)
	Login.
Log in again to ICON-NMR Routine Spectroscopy
Main program menu screen looks like this.
	The program will automatically shim the sample.
Once shimmed the FID will be collected
	The FID will be transformed, phased and integrated for you and a hardcopy will be printed.
To run another sample, select Continue